The survey indicated that many of the people is this region of Raipur have either dental or skeletal fluorosis. A study has been carried out for the determination of fluoride in drinking water in selected area of Raipur. Fluoride was determined by using SPAND reagent and acid zirconium chloride by spectrophotometer of 570 nm. The value range from 0.6 mg/L to 5.83 mg/L. Most of the city have higher concentration of fluoride than suggested by WHO and BIS and most of the people were affected by fluorosis like dental fluorosis or skeletal fluorosis. After the analysis of sample is this region. It was found that high 60 percent of citizen are prone to fluorosis which caused by excess fluoride concentration in drinking water.